Octahydrobenzo[3,4]cyclobuta[1,2-c]furan-1,3-dione

Base Information

• Chemical Name: Octahydrobenzo[3,4]cyclobuta[1,2-c]furan-1,3-dione
• CAS No.: 6537-93-5
• Molecular Formula: C10H12 O3
• Molecular Weight: 180.203
• DSSTox Substance ID: DTXSID50706000
• Mol file: 6537-93-5.mol

Synonyms:6537-93-5;Octahydrobenzo[3,4]cyclobuta[1,2-c]furan-1,3-dione;DTXSID50706000;BICYCLO[4.2.0]OCTANE-7,8-DICARBOXYLIC ANHYDRIDE

Chemical Property of Octahydrobenzo[3,4]cyclobuta[1,2-c]furan-1,3-dione

Chemical Property:

• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 180.078644241
• Heavy Atom Count: 13
• Complexity: 256

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2C(C1)C3C2C(=O)OC3=O

Technology Process of Octahydrobenzo[3,4]cyclobuta[1,2-c]furan-1,3-dione

There total 4 articles about Octahydrobenzo[3,4]cyclobuta[1,2-c]furan-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

maleic anhydride (108-31-6) + benzophenone (119-61-9) + cyclohexene (110-83-8) → 1,1-Diphenylmethanol (91-01-0) + bicyclohexyl-2,2'-diene (1541-20-4) + tetraphenylethane-1,2-diol (464-72-2) + (1-cyclohexen-3-yl)diphenylmethanol (5723-84-2) + bicyclo<4.2.0>octane-7,8-dicarboxylate anhydride (6537-93-5) + 7,7-diphenylhept-6-enal (77083-34-2)

Guidance literature:

In acetonitrile; Product distribution; Irradiation; variation of reaction time;

DOI:10.1016/0040-4039(80)80184-5

Reference yield:

cyclohexene (110-83-8) → bicyclohexyl-2,2'-diene (1541-20-4) + (1-cyclohexen-3-yl)diphenylmethanol (5723-84-2) + bicyclo<4.2.0>octane-7,8-dicarboxylate anhydride (6537-93-5) + 7,7-diphenylhept-6-enal (77083-34-2)

Guidance literature:

With maleic anhydride; benzophenone; Yield given. Further byproducts given. Yields of byproduct given; Irradiation;

DOI:10.1016/0040-4039(80)80184-5

Reference yield:

maleic anhydride (108-31-6) + cyclohexene (110-83-8) → bicyclohexyl-2,2'-diene (1541-20-4) + (1-cyclohexen-3-yl)diphenylmethanol (5723-84-2) + bicyclo<4.2.0>octane-7,8-dicarboxylate anhydride (6537-93-5) + 7,7-diphenylhept-6-enal (77083-34-2)

Guidance literature:

With benzophenone; Yield given. Further byproducts given. Yields of byproduct given; Irradiation;

DOI:10.1016/0040-4039(80)80184-5

upstream raw materials:

maleic anhydride

benzophenone

cyclohexene