2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine

Base Information

Chemical Name:2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine
CAS No.:1245706-91-5
Molecular Formula:C₁₈H₁₄BFN₂
Molecular Weight:288.132
Hs Code.:

Synonyms:2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine

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Chemical Property of 2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine

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Technology Process of 2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine

There total 2 articles about 2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 405-99-2
para-fluorostyrene

: 5656-71-3
2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1245706-91-5
2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine

Guidance literature:: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In dioxane; under N2 atm.; mixt. of p-F-styrene, C10H9N2B and Rh complex in dioxane stirred at 60°C for 4 h;
DOI:10.1246/cl.2010.558

Reference yield:

: 479-27-6
naphthalene-1,8-diamine

: 460748-43-0
(E)-2-(4-fluorophenyl)vinylboronic acid

: 1245706-91-5
2-[(E)-2-(4-fluorophenyl)ethenyl]-2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborine

Guidance literature:: With 1H-imidazole; iron(III) chloride; In water; acetonitrile; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jacs.5b09773