(Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

Base Information

Chemical Name:(Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate
CAS No.:1616924-44-7
Molecular Formula:C₁₈H₂₄N₂O₄
Molecular Weight:332.4
Hs Code.:

Synonyms:(Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

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Chemical Property of (Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

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Technology Process of (Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

There total 5 articles about (Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.17%

: 1616924-43-6
N-hydroxy-2-(8-phenyl-1,4-dioxaspiro[4.5]dec-8-yl)acetamidine

: 108-24-7
acetic anhydride

: 1616924-44-7
(Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

Guidance literature:: at 20 ℃; for 16h;

Reference yield:

: 60356-11-8
cyano(1,4-dioxaspiro[4.5]dec-8-ylidene)acetic acid ethyl ester

: 1616924-44-7
(Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide / tetrahydrofuran; dibutyl ether / 2 h / -78 - -30 °C

1.2: 1 h / -78 - -30 °C

2.1: sodium iodide / dimethyl sulfoxide / 3 h / 150 °C / Sealed tube

2.2: 16 h / 20 °C

3.1: hydroxylamine / ethanol; water / 16 h / 60 °C

4.1: 16 h / 20 °C

With copper(l) iodide; hydroxylamine; sodium iodide; In tetrahydrofuran; ethanol; dibutyl ether; water; dimethyl sulfoxide;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1616924-44-7
(Z)-(1-amino-2-{8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl}ethylidene)amino acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; ammonium acetate / toluene / 16 h / Dean-Stark; Reflux

2.1: copper(l) iodide / tetrahydrofuran; dibutyl ether / 2 h / -78 - -30 °C

2.2: 1 h / -78 - -30 °C

3.1: sodium iodide / dimethyl sulfoxide / 3 h / 150 °C / Sealed tube

3.2: 16 h / 20 °C

4.1: hydroxylamine / ethanol; water / 16 h / 60 °C

5.1: 16 h / 20 °C

With copper(l) iodide; ammonium acetate; hydroxylamine; acetic acid; sodium iodide; In tetrahydrofuran; ethanol; dibutyl ether; water; dimethyl sulfoxide; toluene;