(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

Base Information

Chemical Name:(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester
CAS No.:1439900-33-0
Molecular Formula:C₂₁H₂₁F₅NO₅P
Molecular Weight:493.367
Hs Code.:

Synonyms:(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

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Chemical Property of (2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

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Technology Process of (2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

There total 10 articles about (2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 220592-67-6
O-phenyl-N-(S)-1-(cyclohexoxycarbonyl)ethylphosphoramidic chloride

: 1439900-33-0
(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 4h; Cooling with ice;

Reference yield: 75.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 41324-79-2
(S)-methyl-2-amino cyclohexyl acetate hydrochloride

: 770-12-7
O-phenyl phosphorodichloridate

: 1439900-33-0
(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

Guidance literature:: (S)-methyl-2-amino cyclohexyl acetate hydrochloride; O-phenyl phosphorodichloridate; With triethylamine; In dichloromethane; at -78 - 0 ℃; for 4.5h;

2,3,4,5,6-pentafluorophenol; With triethylamine; In dichloromethane; at 0 ℃; for 4.33h;
DOI:10.1021/acsmedchemlett.6b00270

Reference yield: 56.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 72873-27-9
(S)-cyclohexyl 2-aminopropanoate

: 1439900-33-0
(2S)-2-(((perfluorophenoxy)(phenoxy)phosphoryl)amino)propionic acid cyclohexyl ester

Guidance literature:: O-phenyl phosphorodichloridate; (S)-cyclohexyl 2-aminopropanoate; With triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.5h; Inert atmosphere;

2,3,4,5,6-pentafluorophenol; With triethylamine tris(hydrogen fluoride); In dichloromethane; at 0 - 20 ℃; for 18h;