5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one

Base Information

• Chemical Name: 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one
• CAS No.: 153258-17-4
• Molecular Formula: C₂₀H₁₆N₂OS
• Molecular Weight: 332.426

Synonyms:5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one

Chemical Property of 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one

There total 10 articles about 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

benzaldehyde (100-52-7) + thiourea (17356-08-0) + chloroacetyl chloride (79-04-9) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one (153258-17-4)

Guidance literature:

benzaldehyde; thiourea; 3,4-dihydronaphthalene-1(2H)-one; With N-methyl-2-oxopyrrolidin-1-ium dihydrogen phosphate; at 90 ℃; Microwave irradiation; Green chemistry;

chloroacetyl chloride; With N-methyl-2-oxopyrrolidin-1-ium dihydrogen phosphate; at 90 ℃; for 0.0333333h; Microwave irradiation; Green chemistry;

DOI:10.1007/s11164-015-2249-1

Reference yield: 98.0%

benzaldehyde (100-52-7) + thiourea (17356-08-0) + chloroacetic acid (79-11-8) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one (153258-17-4)

Guidance literature:

benzaldehyde; thiourea; 3,4-dihydronaphthalene-1(2H)-one; With N-methyl-2-oxopyrrolidin-1-ium dihydrogen phosphate; at 90 ℃; Microwave irradiation; Green chemistry;

chloroacetic acid; With N-methyl-2-oxopyrrolidin-1-ium dihydrogen phosphate; at 90 ℃; for 0.0333333h; Temperature; Reagent/catalyst; Catalytic behavior; Microwave irradiation; Green chemistry;

DOI:10.1007/s11164-015-2249-1

Reference yield: 81.6%

3,4,6,7-tetrahydro-4-phenylbenzoquinazolin-2(1H)-thione (85660-18-0) + chloroacetic acid (79-11-8) → 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one (153258-17-4)

Guidance literature:

With sodium acetate; acetic anhydride; acetic acid; at 110 ℃; for 10h;

upstream raw materials:

3,4,6,7-tetrahydro-4-phenylbenzoquinazolin-2(1H)-thione

chloroacetic acid

benzaldehyde

2-benzylidene-1-tetralone

Downstream raw materials:

(Z)-3-(5-((9-oxo-7-phenyl-5H-benzo[h]thiazolo[2,3-b]quinazolin-10(6H,7H,9H)-ylidene)methyl)furan-2-yl)benzoic acid

(E)-10-(4-chlorobenzylidene)-7-phenyl-7,10-dihydro-5H-benzo[h]thiazolo[2,3-b]quinazolin-9(6H)-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 153258-17-4 5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send