isotetrasilane

Base Information

Chemical Name:isotetrasilane
CAS No.:13597-87-0
Molecular Formula:H₁₀Si₄
Molecular Weight:122.421
Hs Code.:
Mol file:13597-87-0.mol

Synonyms:isotetrasilane

Suppliers and Price of isotetrasilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of isotetrasilane

Chemical Property:

Melting Point:-99°C
Refractive Index:1.5449
Boiling Point:101°C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of isotetrasilane

There total 5 articles about isotetrasilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 7440-09-7
potassium

: 7440-21-3
monosilane

: 135524-36-6
Nonafluorobutansulfonsaeure-silylester

: 7783-26-8,134303-33-6
trisilane

: 1590-87-0
disilane

: 13597-87-0
isotetrasilane

: 15947-57-6
neopentasilane

Guidance literature:: In diethylene glycol dimethyl ether; byproducts: H2; further intermediate: KSiH3; under N2, dispersion of potassium reacts with SiH4 at 100°C, concd. in vacuo at 30°C, C4F9SO3SiH3 added at -60°C, stored at this temp. for 10 min, warmed to 40°C; volatiles removed over 3 h in vacuo, SiH4 removed; GC;

Reference yield: 55.0%

: 7440-23-5
sodium

: 7440-21-3
monosilane

: 135524-36-6
Nonafluorobutansulfonsaeure-silylester

: 7783-26-8,134303-33-6
trisilane

: 1590-87-0
disilane

: 13597-87-0
isotetrasilane

: 15947-57-6
neopentasilane

Guidance literature:: In diethylene glycol dimethyl ether; byproducts: H2; further intermediate: NaSiH3; under N2, dispersion of sodium reacts with SiH4 at 100°C, concd. in vacuo at 30°C, C4F9SO3SiH3 added at -60°C, stored at this temp. for 10 min, warmed to 40°C; volatiles removed over 3 h in vacuo, SiH4 removed; GC;

Reference yield: 50.0%

: 7440-09-7
potassium

: 7440-21-3
monosilane

: 98-11-3
benzenesulfonic acid

: 7783-26-8,134303-33-6
trisilane

: 1590-87-0
disilane

: 13597-87-0
isotetrasilane

Guidance literature:: In diethylene glycol dimethyl ether; byproducts: H2; further intermediate: KSiH3; under N2, dispersion of potassium reacts with SiH4 at 100°C, soln. of PhSO3H added dropwise at -40°C; volatiles removed at room temp. in vacuo, SiH4 removed; GC;