Technology Process of C27H27ClN6O3S
There total 5 articles about C27H27ClN6O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: trichlorophosphate / pyridine / 0.5 h
2: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 50 °C
3: tin(ll) chloride / ethyl acetate / 0.5 h / Heating / reflux
4: tetrahydrofuran / 0.5 h / 20 °C
5: hydrogen sulfide / pyridine
6: lithium hydroxide; water / methanol
7: acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile
With
lithium hydroxide; hydrogen sulfide; water; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tin(ll) chloride; trichlorophosphate;
In
tetrahydrofuran; pyridine; methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen sulfide / pyridine
2: lithium hydroxide; water / methanol
3: acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile
With
lithium hydroxide; hydrogen sulfide; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
pyridine; methanol; N,N-dimethyl-formamide; acetonitrile;