N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

Base Information

Chemical Name:N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide
CAS No.:380430-61-5
Molecular Formula:C₁₄H₂₀BNO₃
Molecular Weight:261.129
Hs Code.:2934999090
European Community (EC) Number:671-678-9
DSSTox Substance ID:DTXSID40397188
Nikkaji Number:J2.529.648F
Wikidata:Q72434663
Mol file:380430-61-5.mol

Synonyms:380430-61-5;N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide;2-acetylaminophenylboronic acid pinacol ester;2-acetylaminophenylboronic acid, pinacol ester;N-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide;2-Acetamidophenylboronic acid pinacol ester;N-[2-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide;2-acetamidophenylboronic acid, pinacol ester;SCHEMBL1797092;DTXSID40397188;FTLANOKZIXLBML-UHFFFAOYSA-N;METHYLALPHA-D-FUCOPYRANOSIDE;MFCD02179480;AKOS015960192;AB11230;AS-3104;ACETAMIDE, N-[2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL]-;2-acetamidobenzeneboronic acid, pinacol ester;CS-0153966;FT-0644546;(2-acetylaminophenyl)boronic acid pinacol ester;A20920;F53215;(2-acetylaminophenyl)boronic acid, pinacol ester;EN300-3270155;2-Acetamidophenylboronic acid pinacol ester, 97%;2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-acetanilide;N-Acetyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)aniline;N-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acetamide;2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl);N-(2-(4,4,5,5-tetramethyl-1.3.2-dioxaborolan-2-yl)phenyl)acetamide

Suppliers and Price of N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Acetylaminophenylboronicacid,pinacolester
1g
$ 75.00

SynQuest Laboratories
2-Acetamidobenzeneboronic acid, pinacol ester
5 g
$ 301.00

SynQuest Laboratories
2-Acetamidobenzeneboronic acid, pinacol ester
1 g
$ 130.00

Sigma-Aldrich
2-Acetamidophenylboronic acid pinacol ester 97%
1g
$ 80.80

Sigma-Aldrich
2-Acetamidophenylboronic acid pinacol ester 97%
5g
$ 277.00

Matrix Scientific
N-[2-(Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide >90%
1g
$ 74.00

Matrix Scientific
N-[2-(Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide >90%
500mg
$ 49.00

Matrix Scientific
N-[2-(Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide >90%
5g
$ 262.00

Crysdot
N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide 96%
5g
$ 215.00

Crysdot
N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide 96%
1g
$ 85.00

Total 39 raw suppliers

Chemical Property of N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

Chemical Property:

Vapor Pressure:2.11E-07mmHg at 25°C
Melting Point:172-176 °C(lit.)
Refractive Index:1.51
Boiling Point:424.2 °C at 760 mmHg
PKA:15.26±0.70(Predicted)
Flash Point:210.3 °C
PSA：47.56000
Density:1.078 g/cm³
LogP:2.01720
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:261.1536237
Heavy Atom Count:19
Complexity:341

Purity/Quality:

97% ^*data from raw suppliers

2-Acetylaminophenylboronicacid,pinacolester ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CC=CC=C2NC(=O)C

Technology Process of N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

There total 6 articles about N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 15826-91-2
acetanilide-d5

: 103-84-4
Acetanilid

: 73183-34-3
bis(pinacol)diborane

: 380430-61-5
N-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

: 1374607-05-2
C₁₄H₁₆⁽²⁾H₄BNO₃

Guidance literature:: With palladium diacetate; toluene-4-sulfonic acid; acetic acid; p-benzoquinone; In α,α,α-trifluorotoluene; at 30 ℃; chemoselective reaction;
DOI:10.1039/c2cc31737k

Reference yield: 74.0%

: 103-84-4
Acetanilid

: 73183-34-3
bis(pinacol)diborane

: 380430-61-5
N-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

Guidance literature:: bis(pinacol)diborane; With 5-methyl-2-(thiophen-3-yl)pyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In tetrahydrofuran; at 20 ℃; for 0.0333333h; Inert atmosphere; Glovebox;

Acetanilid; In tetrahydrofuran; at 80 ℃; for 24h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.0c13415