N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine

Base Information

• Chemical Name: N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine
• CAS No.: 1239982-10-5
• Molecular Formula: C₂₆H₃₉NO₃
• Molecular Weight: 413.601
• Mol file: 1239982-10-5.mol

Synonyms:N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine

Chemical Property of N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine

There total 2 articles about N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-tert-Butyl-4-methylphenol (2409-55-4) + ethanolamine (141-43-5) → N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine (1239982-10-5)

Guidance literature:

In methanol; for 24h; Reflux;

DOI:10.1021/acs.inorgchem.0c01202

Reference yield:

HOCH2CH2N(CH2C6H2(OH)(CH3)(C(CH3)3))2*HCl (1286202-36-5) → N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine (1239982-10-5)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water;

DOI:10.1002/ejic.201001251

Reference yield: 92.0%

N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine (1239982-10-5) + phenyltin trichloride (1124-19-2) + acetone (67-64-1) → C32H43NO4Sn*C3H6O

Guidance literature:

N-(1-ethanol)-N,N-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)amine; With methanol; sodium; for 1h; Reflux;

phenyltin trichloride; In tetrahydrofuran; for 1h; Reflux;

acetone;

DOI:10.1021/acs.inorgchem.0c01202

upstream raw materials:

formaldehyd

2-tert-Butyl-4-methylphenol

ethanolamine

HOCH₂CH₂N(CH₂C₆H₂(OH)(CH₃)(C(CH₃)3))2*HCl