C₁₆H₁₈N₂O₃

Base Information

Chemical Name:C₁₆H₁₈N₂O₃
CAS No.:1373618-68-8
Molecular Formula:C₁₆H₁₈N₂O₃
Molecular Weight:286.331
Hs Code.:

C<sub>16</sub>H<sub>18</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₆H₁₈N₂O₃

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Chemical Property of C₁₆H₁₈N₂O₃

Chemical Property:

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Technology Process of C₁₆H₁₈N₂O₃

There total 4 articles about C₁₆H₁₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-56-1
methanol

: 199477-91-3
N-(2-phenylethyl)pyridine-2-carboxamide

: 1373618-68-8
C₁₆H₁₈N₂O₃

Guidance literature:: With [bis(acetoxy)iodo]benzene; palladium diacetate; In para-xylene; at 110 ℃; for 4h; under 760.051 Torr; sealed tube; Inert atmosphere;
DOI:10.1021/ja3023972

Reference yield: 92.0%

: 67-56-1
methanol

: 1181028-82-9
C₁₅H₁₆N₂O₂

: 1373618-68-8
C₁₆H₁₈N₂O₃

Guidance literature:: With [bis(acetoxy)iodo]benzene; palladium diacetate; In para-xylene; at 110 ℃; for 4h; under 760.051 Torr; sealed tube; Inert atmosphere;
DOI:10.1021/ja3023972

Reference yield:

: 98-98-6
2-Picolinic acid

: 64-04-0
phenethylamine

: 1373618-68-8
C₁₆H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: [bis(acetoxy)iodo]benzene; palladium diacetate / para-xylene / 4 h / 110 °C / 760.05 Torr / sealed tube; Inert atmosphere

With [bis(acetoxy)iodo]benzene; palladium diacetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; para-xylene;
DOI:10.1021/ja3023972