3,3-Dimethoxy-2-propenenitrile

Base Information

• Chemical Name: 3,3-Dimethoxy-2-propenenitrile
• CAS No.: 15732-02-2
• Molecular Formula: C5H7NO2
• Molecular Weight: 113.116
• Hs Code.: 2926909090
• Mol file: 15732-02-2.mol

Synonyms:Acrylonitrile,3-oxo-, dimethyl acetal (8CI);Cyanoketene dimethyl acetal;

Chemical Property of 3,3-Dimethoxy-2-propenenitrile

Chemical Property:

• Vapor Pressure: 0.0645mmHg at 25°C
• Melting Point: 41.5-42 °C
• Refractive Index: 1.429
• Boiling Point: 230.8 °C at 760 mmHg
• Flash Point: 107.6 °C
• PSA: 42.25000
• Density: 1.022 g/cm³
• LogP: 0.64418

Purity/Quality:

99.90% ^*data from raw suppliers

3,3-Dimethoxyacrylonitrile 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3-Dimethoxy-2-propenenitrile

There total 3 articles about 3,3-Dimethoxy-2-propenenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-cyano-1,1,1-trimethoxyethane (70138-31-7) → 1-cyano-2,2-bis(methoxy)ethylene (15732-02-2)

Guidance literature:

at 220 - 225 ℃;

DOI:10.1021/ja01169a014

Reference yield:

3,3-dichloro-acrylonitrile (7436-85-3) + sodium methylate (124-41-4) → 1-cyano-2,2-bis(methoxy)ethylene (15732-02-2)

Guidance literature:

DOI:10.1021/jo00821a026

Reference yield:

→ 1-cyano-2,2-bis(methoxy)ethylene (15732-02-2)

Guidance literature:

β,β-Dichloracrylnitril, CH3OH;

DOI:10.1021/jo00828a068

upstream raw materials:

2-cyano-1,1,1-trimethoxyethane

3,3-dichloro-acrylonitrile

sodium methylate

Downstream raw materials:

methyl 2-bromo-2-cyanoacetate

methyl 2-benzyl-2-cyano-3-phenylpropionate

methyl 2-cyano-4-phenylpropanoate

Ethyl methyl ethylphosphonate

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