8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Base Information

Chemical Name:8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine
CAS No.:1345983-71-2
Molecular Formula:C₂₄H₃₀BrNOS
Molecular Weight:460.478
Hs Code.:

Synonyms:8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Suppliers and Price of 8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

There total 13 articles about 8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.7%

: 1345983-70-1
[2-[(2-amino-2-butylhexanyl)thio]-4-bromo-5-(methyloxy)phenyl](phenyl)methanone

: 1345983-71-2
8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Guidance literature:: With citric acid; In toluene; at 130 ℃; for 50h; Reflux;

Reference yield:

: 393855-78-2
2-amino-2-butyl-hexanoic acid ethyl ester

: 1345983-71-2
8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 65 °C

1.2: 2 h / 0 °C

2.1: chlorosulfonic acid / ethyl acetate / 3 h / 25 - 40 °C

3.1: potassium hydroxide / ethanol; water / 18 h / 70 °C / Reflux

3.2: 15 h / 85 °C

4.1: citric acid / toluene / 50 h / 130 °C / Reflux

With chlorosulfonic acid; lithium aluminium tetrahydride; citric acid; potassium hydroxide; In tetrahydrofuran; ethanol; water; ethyl acetate; toluene;

Reference yield:

: 1345983-66-5
S-[5-bromo-4-(methyloxy)-2-(phenylcarbonyl)phenyl]diethylthiocarbamate

: 1345983-71-2
8-bromo-3,3-dibutyl-7-(methyloxy)-5-phenyl-2,3-dihydro-1,4-benzothiazepine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol; water / 18 h / 70 °C / Reflux

1.2: 15 h / 85 °C

2.1: citric acid / toluene / 50 h / 130 °C / Reflux

With citric acid; potassium hydroxide; In ethanol; water; toluene;