Tetraamminepalladium(II) chloride monohydrate

Base Information

• Chemical Name: Tetraamminepalladium(II) chloride monohydrate
• CAS No.: 13933-31-8
• Molecular Formula: 2Cl*H₂O*H₁₂N₄Pd
• Molecular Weight: 263.463
• Mol file: 13933-31-8.mol

Synonyms:Palladium(2+),tetraammine-, dichloride, monohydrate (8CI);Tetraamminepalladium dichloride,hydrate (7CI);Tetraamminepalladium(2+) dichloride monohydrate;palladium(2+) chloride ammoniate hydrate (1:2:4:1);

Chemical Property of Tetraamminepalladium(II) chloride monohydrate

Chemical Property:

• Melting Point: 120 °C (dec.)(lit.)
• PSA: 22.19000
• Density: 1.91 g/mL at 25 °C(lit.)
• LogP: 2.61030
• Storage Temp.: Sealed in dry,Room Temperature
• Sensitive.: Hygroscopic
• Water Solubility.: Soluble in water.

Purity/Quality:

98% ^*data from raw suppliers

Tetraamminepalladium(II) chloride monohydrate ≥99.99% trace metals basis ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Tetraamminepalladium(II) chloride monohydrate is used to prepare trans-diamminedichloropalladium(II). It is also utilized in the preparation of mesoporous carbon supporting palladium nanoparticles by using graphite oxide. It is used as catalysts, reagents, and analytical reagents.

Technology Process of Tetraamminepalladium(II) chloride monohydrate

There total 5 articles about Tetraamminepalladium(II) chloride monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diamminedichloropalladium(II) (14323-43-4,15684-18-1,13782-33-7) + ammonia (7664-41-7) + water (7732-18-5) → tetraamminepalladium(II) chloride monohydrate (13933-31-8)

Guidance literature:

In ammonia; reactn. of (Pd(NH3)2Cl2) (wetted with ethanol) with concd. NH3 soln.; evaporization of soln. at 90 °C; pptn. of Pd(NH3)4Cl2*H2O and Pd(NH3)2Cl2;;

Reference yield:

tetramminepalladium(II) chloride (13815-17-3) + water (7732-18-5) → tetraamminepalladium(II) chloride monohydrate (13933-31-8)

Guidance literature:

In ammonia; aq. ammonia=NH3; on evaporization of soln.;

Reference yield:

cis-dichloro(ethylenediamine)palladium(II) (15020-99-2) + water (7732-18-5) → tetraamminepalladium(II) chloride monohydrate (13933-31-8)

Guidance literature:

With C₂H₄(SC₂H₅)2; byproducts: (Pd(C2H4(SC2H5)2Cl2); react. of C2H4(SC2H5)2 with (PdenCl2);; impurity: (Pd(C2H4(SC2H5)2)Cl2);;

upstream raw materials:

tetramminepalladium(II) chloride

water

Vauquelin's salt

cis-dichloro(ethylenediamine)palladium(II)

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