N⁴-(pivaloyl)-N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone

Base Information

• Chemical Name: N⁴-(pivaloyl)-N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone
• CAS No.: 1430730-67-8
• Molecular Formula: C₄₇H₄₅N₃O₁₂S
• Molecular Weight: 875.953
• Mol file: 1430730-67-8.mol

Synonyms:N⁴-(pivaloyl)-N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone

Chemical Property of N⁴-(pivaloyl)-N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁴-(pivaloyl)-N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone

There total 4 articles about N⁴-(pivaloyl)-N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

N1-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone (1430730-32-7) + pivaloyl chloride (3282-30-2) → N4-(pivaloyl)-N1-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone (1430730-67-8)

Guidance literature:

With pyridine; dmap; In chloroform; at 20 ℃; Reflux;

Reference yield:

toluene-4-sulfonic acid hydrazide (1576-35-8) → N4-(pivaloyl)-N1-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone (1430730-67-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 72 h / 20 °C

2: pyridine; dmap / chloroform / 20 °C / Reflux

With pyridine; dmap; In dichloromethane; chloroform;

Reference yield:

ethyl C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formimidate (1430730-28-1) → N4-(pivaloyl)-N1-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone (1430730-67-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 72 h / 20 °C

2: pyridine; dmap / chloroform / 20 °C / Reflux

With pyridine; dmap; In dichloromethane; chloroform;

upstream raw materials:

toluene-4-sulfonic acid hydrazide

N¹-tosyl-C-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)formamidrazone

pivaloyl chloride

2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonamide

Downstream raw materials:

3-(tert-butyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole