3-methoxyphenylhydrazone of 2,3-piperidinedione

Base Information

Chemical Name:3-methoxyphenylhydrazone of 2,3-piperidinedione
CAS No.:97456-64-9
Molecular Formula:C₁₂H₁₅N₃O₂
Molecular Weight:233.27
Hs Code.:

Synonyms:3-methoxyphenylhydrazone of 2,3-piperidinedione

Suppliers and Price of 3-methoxyphenylhydrazone of 2,3-piperidinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-methoxyphenylhydrazone of 2,3-piperidinedione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-methoxyphenylhydrazone of 2,3-piperidinedione

There total 5 articles about 3-methoxyphenylhydrazone of 2,3-piperidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 41907-06-6
piperidinedione

: 15384-39-1
(3-methoxyphenyl)hydrazine

: 97456-64-9
3-methoxyphenylhydrazone of 2,3-piperidinedione

Guidance literature:: In ethanol; dichloromethane; for 0.25h; Heating;

Reference yield:

: 19365-08-3,220928-01-8
3-hydroxypiperidin-2-one

: 97456-64-9
3-methoxyphenylhydrazone of 2,3-piperidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, 15 min, 2.) room temperature

2: 78 percent / ethanol; CH₂Cl₂ / 0.25 h / Heating

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane;