(borane)diphenylphosphinomethyl sulfonate

Base Information

Chemical Name:(borane)diphenylphosphinomethyl sulfonate
CAS No.:815577-64-1
Molecular Formula:C₁₄H₁₈BO₃PS
Molecular Weight:308.146
Hs Code.:

Synonyms:(borane)diphenylphosphinomethyl sulfonate

Suppliers and Price of (borane)diphenylphosphinomethyl sulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (borane)diphenylphosphinomethyl sulfonate

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (borane)diphenylphosphinomethyl sulfonate

There total 4 articles about (borane)diphenylphosphinomethyl sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 127686-81-1
hydroxymethyl(diphenyl)phosphine borane complex

: 124-63-0
methanesulfonyl chloride

: 815577-64-1
(borane)diphenylphosphinomethyl sulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 15h;
DOI:10.1021/ol048271s

Reference yield:

: 829-85-6
diphenylphosphane

: 815577-64-1
(borane)diphenylphosphinomethyl sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: BH₃*Me₂S / tetrahydrofuran / 2 h

1.2: 100 percent / KOH / H₂O; tetrahydrofuran / 4 h

2.1: 78 percent / Et₃N / CH₂Cl₂ / 15 h / 0 °C

With dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol048271s

Reference yield:

: 41593-58-2
diphenylphosphineborane

: 815577-64-1
(borane)diphenylphosphinomethyl sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / tetrahydrofuran; water / 2 h

2: triethylamine / dichloromethane / 15 h / 0 °C / Inert atmosphere

With triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/anie.201611415