hydroxymethyl(diphenyl)phosphine borane complex

Base Information

Chemical Name:hydroxymethyl(diphenyl)phosphine borane complex
CAS No.:127686-81-1
Molecular Formula:C₁₃H₁₆BOP
Molecular Weight:230.054
Hs Code.:

Synonyms:hydroxymethyl(diphenyl)phosphine borane complex

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Chemical Property of hydroxymethyl(diphenyl)phosphine borane complex

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Technology Process of hydroxymethyl(diphenyl)phosphine borane complex

There total 4 articles about hydroxymethyl(diphenyl)phosphine borane complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 829-85-6
diphenylphosphane

: 127686-81-1
hydroxymethyl(diphenyl)phosphine borane complex

Guidance literature:: diphenylphosphane; With dimethylsulfide borane complex; In tetrahydrofuran; for 2h;

formaldehyd; With potassium hydroxide; In tetrahydrofuran; water; for 4h;
DOI:10.1021/ol048271s

Reference yield: 90.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 41593-58-2
diphenylphosphineborane

: 127686-81-1
hydroxymethyl(diphenyl)phosphine borane complex

Guidance literature:: With potassium hydroxide; In methanol; 0°C, stirring; treatment with aq. HCl, extn. (ether), preparative TLC;
DOI:10.1021/ja00169a036

Reference yield:

: 829-85-6
diphenylphosphane

: 127686-81-1
hydroxymethyl(diphenyl)phosphine borane complex

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / Inert atmosphere

2: potassium hydroxide / tetrahydrofuran; water / 2 h

With potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1002/anie.201611415