C₃₂H₃₀N₂O₃

Base Information

Chemical Name:C₃₂H₃₀N₂O₃
CAS No.:1256489-02-7
Molecular Formula:C₃₂H₃₀N₂O₃
Molecular Weight:490.602
Hs Code.:

C<sub>32</sub>H<sub>30</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₃₂H₃₀N₂O₃

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Chemical Property of C₃₂H₃₀N₂O₃

Chemical Property:

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Technology Process of C₃₂H₃₀N₂O₃

There total 8 articles about C₃₂H₃₀N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1256489-01-6
C₃₂H₂₈N₂O₂

: 1256489-02-7
C₃₂H₃₀N₂O₃

Guidance literature:: hydrido(dimethylphosphinous acid-κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); In ethanol; at 85 ℃;

Reference yield:

: 52200-49-4
3-bromo-2-(phenylmethoxy)pyridine

: 1256489-02-7
C₃₂H₃₀N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: potassium acetate; bis(pinacol)diborane / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 26 h / 70 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / methanol; dichloromethane / 0.5 h / 115 °C / Sealed tube; Microwave Irradiation

3: sodium methylate / methanol / -78 - 20 °C

4: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 3 h / 75 °C

5: hydrido(dimethylphosphinous acid-κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / ethanol / 85 °C

With copper(l) iodide; sodium methylate; potassium acetate; sodium carbonate; triethylamine; bis(pinacol)diborane; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrido(dimethylphosphinous acid-κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 24623-65-2
3-tert-butyl-2-hydroxybenzaldehyde

: 1256489-02-7
C₃₂H₃₀N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / dichloromethane / 1.5 h / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 50 °C

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / methanol; dichloromethane / 0.5 h / 115 °C / Sealed tube; Microwave Irradiation

4: sodium methylate / methanol / -78 - 20 °C

5: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 3 h / 75 °C

6: hydrido(dimethylphosphinous acid-κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / ethanol / 85 °C

With copper(l) iodide; bromine; sodium methylate; sodium carbonate; potassium carbonate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrido(dimethylphosphinous acid-κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;