tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

Base Information

Chemical Name:tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate
CAS No.:1439362-14-7
Molecular Formula:C₃₃H₃₇BrN₂O₂
Molecular Weight:573.573
Hs Code.:

Synonyms:tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

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Technology Process of tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

There total 7 articles about tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1216944-04-5
tert-butyl 3-(naphthalen-1-ylmethylamino)propylcarbamate

: 20248-86-6
4-4'-bis(bromomethyl)biphenyl

: 1439362-14-7
tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 20 ℃;
DOI:10.1002/cmdc.201200390

Reference yield:

: 1439361-95-1
tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

: 1439362-14-7
tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; thiophenol / N,N-dimethyl-formamide / 2 h / 20 °C

2: potassium iodide; potassium carbonate / acetonitrile / 20 °C

With potassium carbonate; thiophenol; potassium iodide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201200390

Reference yield:

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1439362-14-7
tert-butyl 3-(((4'-(bromomethyl)biphenyl-4-yl)methyl)(naphthalen-1-ylmethyl)amino)propylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

2: potassium carbonate; thiophenol / N,N-dimethyl-formamide / 2 h / 20 °C

3: potassium iodide; potassium carbonate / acetonitrile / 20 °C

With potassium carbonate; thiophenol; potassium iodide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201200390