4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Base Information

Chemical Name:4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid
CAS No.:355017-64-0
Molecular Formula:C12H15 N O7
Molecular Weight:285.254
Hs Code.:2918990090
European Community (EC) Number:846-650-6
DSSTox Substance ID:DTXSID10401463
Nikkaji Number:J3.105.365J
Mol file:355017-64-0.mol

Synonyms:355017-64-0;4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid;4-[4-(hydroxymethyl)-2-methoxy-5-nitrophenoxy]butanoic acid;4-(4-Hydroxymethyl-2-methoxy-5-nitrophenoxy)butyric acid;4-(4-HYDROXYMETHYL-2-METHOXY-5-NITRO-PHENOXY)BUTYRIC ACID;SCHEMBL329986;DTXSID10401463;MYBBGZZXDFIZGU-UHFFFAOYSA-N;CS-0260334;F83370;H-6830;EN300-7493941;4-(4-HYDROXYMETHYL-2-METHOXY-5-NITROPHENOXY)BUTYRICACID

Suppliers and Price of 4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid 95+%
1g
$ 588.00

Matrix Scientific
4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid 95+%
250mg
$ 265.00

Crysdot
4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoicacid 95+%
5g
$ 823.00

American Custom Chemicals Corporation
4-(4-HYDROXYMETHYL-2-METHOXY-5-NITROPHENOXY)BUTYRIC ACID 95.00%
1G
$ 808.50

American Custom Chemicals Corporation
4-(4-HYDROXYMETHYL-2-METHOXY-5-NITROPHENOXY)BUTYRIC ACID 95.00%
500MG
$ 739.20

AK Scientific
4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoicacid
1g
$ 843.00

Total 13 raw suppliers

Chemical Property of 4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Chemical Property:

Melting Point:178-182 ºC
PSA：121.81000
LogP:1.86250
XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:285.08485182
Heavy Atom Count:20
Complexity:330

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)CO)[N+](=O)[O-])OCCCC(=O)O

Technology Process of 4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

There total 11 articles about 4-(4-(Hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 176375-43-2
methyl 4-(4-(hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoate

: 355017-64-0
4-(4-(hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Guidance literature:: With water; potassium hydroxide; In methanol; at 20 ℃; for 2h;
DOI:10.1039/c9cc09449k

Reference yield: 90.0%

: 263758-69-6
4-(4-formyl-2-methoxy-5-nitrophenoxy)butanoic acid

: 355017-64-0
4-(4-(hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Guidance literature:: With sodium tetrahydroborate; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja305280w

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 355017-64-0
4-(4-(hydroxymethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2: nitric acid / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / water / 3 h / 90 °C / Inert atmosphere

4: sodium tetrahydroborate / 12 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; nitric acid; potassium carbonate; trifluoroacetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1021/ja305280w