Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

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Chemical Name:Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester
CAS No.:210166-27-1
Molecular Formula:C₄₀H₃₇IO₈
Molecular Weight:772.633
Hs Code.:

Synonyms:Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

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Chemical Property of Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

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Technology Process of Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

There total 6 articles about Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 67-56-1
methanol

: 210166-26-0
Acetic acid 3,5-bis-benzyloxy-2-[(E)-3-(4-benzyloxy-phenyl)-acryloyl]-6-iodo-phenyl ester

: 210166-27-1
Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

Guidance literature:: With thallium(III) nitrate; In chloroform; at 40 ℃; for 7h;

Reference yield:

: 18065-05-9
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

: 210166-27-1
Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 76 percent / silver trifluoroacetate, I₂ / CHCl₃ / 0.5 h / Ambient temperature

2: 90 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 1.25 h / Ambient temperature

3: KOH / ethanol / 4.5 h / Heating

4: conc. aq. HCl / CHCl₃; ethanol / 1 h / 40 °C

5: 94 percent / pyridine / 2 h / 110 °C

6: 69 percent / thallium (III) nitrate trihydrate / CHCl₃ / 7 h / 40 °C

With pyridine; hydrogenchloride; potassium hydroxide; iodine; silver trifluoroacetate; N-ethyl-N,N-diisopropylamine; thallium(III) nitrate; In ethanol; dichloromethane; chloroform;

Reference yield:

: 95165-66-5
3-Iod-2-hydroxy-4,6-dibenzyloxy-acetophenon

: 210166-27-1
Acetic acid 3,5-bis-benzyloxy-2-[2-(4-benzyloxy-phenyl)-3,3-dimethoxy-propionyl]-6-iodo-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 1.25 h / Ambient temperature

2: KOH / ethanol / 4.5 h / Heating

3: conc. aq. HCl / CHCl₃; ethanol / 1 h / 40 °C

4: 94 percent / pyridine / 2 h / 110 °C

5: 69 percent / thallium (III) nitrate trihydrate / CHCl₃ / 7 h / 40 °C

With pyridine; hydrogenchloride; potassium hydroxide; N-ethyl-N,N-diisopropylamine; thallium(III) nitrate; In ethanol; dichloromethane; chloroform;