epi-3-aminonocardicin tert-butyl ester hydrochloride

Base Information

Chemical Name:epi-3-aminonocardicin tert-butyl ester hydrochloride
CAS No.:1443793-33-6
Molecular Formula:C₁₅H₂₀N₂O₄*ClH
Molecular Weight:328.796
Hs Code.:

Synonyms:epi-3-aminonocardicin tert-butyl ester hydrochloride

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Chemical Property of epi-3-aminonocardicin tert-butyl ester hydrochloride

Chemical Property:

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Technology Process of epi-3-aminonocardicin tert-butyl ester hydrochloride

There total 4 articles about epi-3-aminonocardicin tert-butyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1443793-29-0
N-(4,6-diphenyl-4-oxazolin-2-onyl)-L-seryl-L-[p-(benzyloxy)phenyl]glycine tert-butyl ester

: 1443793-33-6
epi-3-aminonocardicin tert-butyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: diethylazodicarboxylate; triethyl phosphite / tetrahydrofuran / 12 h / 20 °C / Darkness

2: 10 wt% Pd(OH)2 on carbon; hydrogen / tetrahydrofuran / 48 h / 2585.81 Torr

3: hydrogenchloride / diethyl ether; water

With hydrogenchloride; 10 wt% Pd(OH)2 on carbon; hydrogen; diethylazodicarboxylate; triethyl phosphite; In tetrahydrofuran; diethyl ether; water;
DOI:10.1021/jo4007893

Reference yield:

: 1443793-30-3
3-N-(4,5-diphenyl-4-oxazolin-2-onyl)-epi-aminonocardicin tert-butyl ester

: 1443793-33-6
epi-3-aminonocardicin tert-butyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 10 wt% Pd(OH)2 on carbon; hydrogen / tetrahydrofuran / 48 h / 2585.81 Torr

2: hydrogenchloride / diethyl ether; water

With hydrogenchloride; 10 wt% Pd(OH)2 on carbon; hydrogen; In tetrahydrofuran; diethyl ether; water;
DOI:10.1021/jo4007893

Reference yield:

: 1443793-28-9
L-[p-(benzyloxy)phenyl]glycine tert-butyl ester toluenesulfonate

: 1443793-33-6
epi-3-aminonocardicin tert-butyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.02 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: diethylazodicarboxylate; triethyl phosphite / tetrahydrofuran / 12 h / 20 °C / Darkness

3.1: 10 wt% Pd(OH)2 on carbon; hydrogen / tetrahydrofuran / 48 h / 2585.81 Torr

4.1: hydrogenchloride / diethyl ether; water

With hydrogenchloride; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; 10 wt% Pd(OH)2 on carbon; hydrogen; N-ethyl-N,N-diisopropylamine; diethylazodicarboxylate; triethyl phosphite; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jo4007893