N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Base Information

Chemical Name:N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
CAS No.:1204742-78-8
Molecular Formula:C₁₄H₂₀BNO₄
Molecular Weight:277.128
Hs Code.:2931900090
DSSTox Substance ID:DTXSID30682212
Wikidata:Q82606518
Mol file:1204742-78-8.mol

Synonyms:1204742-78-8;N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide;4-(O-Methylhydroxylaminocarbonyl)phenylboronic acid, pinacol ester;SCHEMBL1558461;DTXSID30682212;XWLLIHOJLBOYHT-UHFFFAOYSA-N;MFCD17015820;AKOS016001034;BS-26014;CS-0175609;FT-0734839;F73109;4-(O-methyl hydroxylaminocarbonyl)phenylboronic acid pinacol ester

Suppliers and Price of N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-(O-Methylhydroxylaminocarbonyl)phenylboronicAcidPinacolEster
10mg
$ 45.00

Crysdot
N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide 95+%
25g
$ 565.00

Chemenu
N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide 98%
5g
$ 178.00

Chemenu
N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide 98%
1g
$ 59.00

American Custom Chemicals Corporation
N-METHOXY-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZAMIDE 95.00%
1G
$ 179.55

Alichem
N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
25g
$ 582.42

AK Scientific
4-(O-Methylhydroxylaminocarbonyl)phenylboronicacidpinacolester
5g
$ 291.00

Total 11 raw suppliers

Chemical Property of N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Chemical Property:

Density:1.11±0.1 g/cm3(Predicted)
Storage Temp.:Room temperature.
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:277.1485383
Heavy Atom Count:20
Complexity:348

Purity/Quality:

97% ^*data from raw suppliers

4-(O-Methylhydroxylaminocarbonyl)phenylboronicAcidPinacolEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CC=C(C=C2)C(=O)NOC

Technology Process of N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

There total 2 articles about N-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72755-10-3
4-bromo-N-methoxybenzamide

: 73183-34-3
bis(pinacol)diborane

: 1204742-78-8
C₁₄H₂₀BNO₄

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 80 ℃;
DOI:10.1016/j.bmcl.2017.06.032

Reference yield:

: 586-75-4
4-chlorobenzoyl chloride

: 1204742-78-8
C₁₄H₂₀BNO₄

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane

2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2017.06.032

Reference yield: 84.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1204742-78-8
C₁₄H₂₀BNO₄

: 203442-83-5
methyl 4-(N-methoxy-N-methylcarbamoyl)benzoate

Guidance literature:: With palladium diacetate; triphenylphosphine; p-benzoquinone; at 20 ℃; for 8h; under 760.051 Torr;
DOI:10.1002/adsc.200900836