4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

Base Information

Chemical Name:4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate
CAS No.:1352246-27-5
Molecular Formula:C₂HF₃O₂*C₁₅H₁₉ClN₄
Molecular Weight:404.82
Hs Code.:

Synonyms:4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

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Chemical Property of 4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

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Technology Process of 4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

There total 3 articles about 4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352246-25-3
tert-butyl 4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine-1-carboxylate

: 76-05-1
trifluoroacetic acid

: 1352246-27-5
4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 84358-13-4,174286-31-8
N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid

: 1352246-27-5
4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: HATU / dichloromethane / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: sodium acetate; acetic acid / 1,4-dioxane / 16 h / 90 °C

3.1: dichloromethane / 16 h / 20 °C

With sodium acetate; acetic acid; HATU; In 1,4-dioxane; dichloromethane;

Reference yield:

: 1352246-24-2
tert-butyl 4-(ethanethioylcarbamoyl)piperidine-1-carboxylate

: 1352246-27-5
4-[1-(4-chloro-3-methylphenyl)-3-methyl-1H-1,2,4-triazol-5-yl]piperidine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; acetic acid / 1,4-dioxane / 16 h / 90 °C

2: dichloromethane / 16 h / 20 °C

With sodium acetate; acetic acid; In 1,4-dioxane; dichloromethane;