N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide

Base Information

• Chemical Name: N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide
• CAS No.: 956468-07-8
• Molecular Formula: C₂₀H₂₆N₂O₈S₂
• Molecular Weight: 486.567

Synonyms:N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide

Chemical Property of N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide

Chemical Property:

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Technology Process of N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide

There total 1 articles about N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3,4-dimethoxybenzene-1-sulfonyl chloride (23095-31-0) + pyrrolidin-3-amine (79286-79-6) → N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide (956468-07-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 2h;

Reference yield: 44.0%

N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide (956468-07-8) + 1-iodo-propane (107-08-4) → N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)-N-propylbenzenesulfonamide (956467-42-8)

Guidance literature:

With potassium carbonate; In acetonitrile; for 36h; Heating / reflux;

Reference yield: 42.0%

N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)benzenesulfonamide (956468-07-8) + Isobutyl iodide (513-38-2) → N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)-N-(2-methylpropyl)benzenesulfonamide (956467-43-9)

Guidance literature:

With potassium carbonate; In acetonitrile; at 82 ℃; for 36h;

upstream raw materials:

3,4-dimethoxybenzene-1-sulfonyl chloride

pyrrolidin-3-amine

Downstream raw materials:

N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)-N-propylbenzenesulfonamide

N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-3,4-bis(methyloxy)-N-(2-methylpropyl)benzenesulfonamide

N-(1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-3-pyrrolidinyl)-N-(cyclobutylmethyl)-3,4-bis(methyloxy)benzenesulfonamide

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