2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Base Information

Chemical Name:2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether
CAS No.:1385773-93-2
Molecular Formula:C₁₈H₂₉N₅O₃
Molecular Weight:363.46
Hs Code.:

Synonyms:2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

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Chemical Property of 2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

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Technology Process of 2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

There total 9 articles about 2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₇N₅O₃

: 1385773-93-2
2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 ℃; for 2h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1385773-93-2
2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 20 °C / Inert atmosphere

2: sodium hydroxide / tetra-(n-butyl)ammonium iodide / dichloromethane; water / Inert atmosphere

3: hydrogen; ammonia / palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 760.05 Torr

4: methanol

5: sodium tetrahydroborate; methanol / 2 h / 0 °C

With methanol; sodium tetrahydroborate; ammonia; hydrogen; sodium hydroxide; palladium on activated charcoal; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 1385773-93-2
2-(t-butoxycarbonylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / tetra-(n-butyl)ammonium iodide / dichloromethane; water / Inert atmosphere

2: hydrogen; ammonia / palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 760.05 Torr

3: methanol

4: sodium tetrahydroborate; methanol / 2 h / 0 °C

With methanol; sodium tetrahydroborate; ammonia; hydrogen; sodium hydroxide; palladium on activated charcoal; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; methanol; dichloromethane; water;