2-(4-chlorophenyl)-N,N-diethylacrylamide

Base Information

Chemical Name:2-(4-chlorophenyl)-N,N-diethylacrylamide
CAS No.:137958-84-0
Molecular Formula:C₁₃H₁₆ClNO
Molecular Weight:237.729
Hs Code.:

Synonyms:2-(4-chlorophenyl)-N,N-diethylacrylamide

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Chemical Property of 2-(4-chlorophenyl)-N,N-diethylacrylamide

Chemical Property:

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Technology Process of 2-(4-chlorophenyl)-N,N-diethylacrylamide

There total 4 articles about 2-(4-chlorophenyl)-N,N-diethylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 873-73-4
4-n-chlorophenylacetylene

: 201230-82-2
carbon monoxide

: 109-89-7
diethylamine

: 23784-71-6
4-Chlor-zimtsaeure-N,N-diethylamid

: 137958-84-0
2-(4-chlorophenyl)-N,N-diethylacrylamide

Guidance literature:: With triphenylphosphine; methyl iodide; bis-triphenylphosphine-palladium(II) chloride; at 120 ℃; for 6h; under 3800 Torr; Title compound not separated from byproducts;
DOI:10.1246/cl.1991.1673

Reference yield: 43.0%

: 873-73-4
4-n-chlorophenylacetylene

: 201230-82-2
carbon monoxide

: 121-44-8
triethylamine

: 137958-84-0
2-(4-chlorophenyl)-N,N-diethylacrylamide

Guidance literature:: With [1,1′-bis(di-cyclohexylphosphino)ferrocene]dichloropalladium (II); di-tert-butyl peroxide; ammonium chloride; In acetonitrile; at 120 ℃; for 24h; under 15201 Torr; regioselective reaction; Autoclave; Schlenk technique;
DOI:10.1021/acs.orglett.7b03331

Reference yield:

: 1878-66-6
4-chlorophenylacetic Acid

: 137958-84-0
2-(4-chlorophenyl)-N,N-diethylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride

2: caesium carbonate

With oxalyl dichloride; caesium carbonate;
DOI:10.1039/c4cy00633j