2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one

Base Information

• Chemical Name: 2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one
• CAS No.: 1127352-16-2
• Molecular Formula: C₂₄H₃₄O₆Si
• Molecular Weight: 446.616

Synonyms:2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one

Chemical Property of 2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one

Chemical Property:

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Technology Process of 2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one

There total 2 articles about 2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

methanol (67-56-1) + tert-butyl(2-methoxy-5-(1-(3,4,5-trimethoxyphenyl)vinyl)phenoxy)dimethylsilane (1067880-35-6) → 2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one (1127352-16-2) + C25H36O6Si

Guidance literature:

With [bis(acetoxy)iodo]benzene; sulfuric acid; at -20 ℃; for 0.5h; Reagent/catalyst;

DOI:10.3390/ijms21051817

Reference yield:

trans-3-(3-tert-butyldimethylsilyloxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)oxirane → 2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one (1127352-16-2)

Guidance literature:

With Amberlist 15; lithium bromide; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1002/ejoc.200800957

Reference yield: 95.0%

2-(3-((tert-butyldimethylsilyl)oxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one (1127352-16-2) → 2-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one (89018-72-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.5h;

DOI:10.3390/ijms21051817

upstream raw materials:

methanol

tert-butyl(2-methoxy-5-(1-(3,4,5-trimethoxyphenyl)vinyl)phenoxy)dimethylsilane

Downstream raw materials:

2-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)ethan-1-one

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