(2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal

Base Information

• Chemical Name: (2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal
• CAS No.: 1018783-17-9
• Molecular Formula: C₁₆H₂₁N₅O₃S₂
• Molecular Weight: 395.506

Synonyms:(2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal

Chemical Property of (2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal

Chemical Property:

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Technology Process of (2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal

There total 1 articles about (2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C12H11N5O4 (1037070-33-9) + ethanethiol (75-08-1) → (2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal (1018783-17-9)

Guidance literature:

With chloro-trimethyl-silane; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2008.04.006

Reference yield:

(2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal (1018783-17-9) + (2S)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-pyrrolidine-2-carboxaldehyde diethyl-dithioacetal (1037070-06-6) → C36H47N7O8S4

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2008.04.006

Reference yield:

(2S,4S)-N-[2-nitrobenzoyl]-4-azidopyrrolidine-2-carboxaldehyde diethylthioacetal (1018783-17-9) + dimethyl acetylenedicarboxylate (762-42-5) → C22H27N5O7S2 (1018783-19-1)

Guidance literature:

In benzene; for 6h; Heating;

DOI:10.1016/j.bmcl.2007.12.063

upstream raw materials:

C₁₂H₁₁N₅O₄

ethanethiol

Downstream raw materials:

C₂₂H₂₇N₅O₇S₂

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