ethyl-phenyl-thiocarbamic acid O-ethyl ester

Base Information

• Chemical Name: ethyl-phenyl-thiocarbamic acid O-ethyl ester
• CAS No.: 83441-23-0
• Molecular Formula: C₁₁H₁₅NOS
• Molecular Weight: 209.312
• Mol file: 83441-23-0.mol

Synonyms:ethyl-phenyl-thiocarbamic acid O-ethyl ester

Chemical Property of ethyl-phenyl-thiocarbamic acid O-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl-phenyl-thiocarbamic acid O-ethyl ester

There total 2 articles about ethyl-phenyl-thiocarbamic acid O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

ethyl-phenyl-carbamic acid ethyl ester (1013-75-8) → ethyl-phenyl-thiocarbamic acid O-ethyl ester (83441-23-0)

Guidance literature:

With Lawessons reagent; In xylene; at 140 ℃; for 24h;

DOI:10.1016/0040-4020(82)85099-0

Reference yield:

sodium ethanolate (141-52-6) + ethyl-phenyl-thiocarbamoyl chloride (35517-93-2) → ethyl-phenyl-thiocarbamic acid O-ethyl ester (83441-23-0)

Guidance literature:

With diethyl ether;

Reference yield: 57.0%

ethyl-phenyl-thiocarbamic acid O-ethyl ester (83441-23-0) → ethyl-phenyl-carbamic acid ethyl ester (1013-75-8)

Guidance literature:

With hydrogenchloride; N-methyl-N-nitrosoaniline; potassium iodide; In dichloromethane; water; at 22 ℃; for 16h;

DOI:10.1016/S0040-4020(01)88548-3

upstream raw materials:

sodium ethanolate

ethyl-phenyl-thiocarbamoyl chloride

ethyl-phenyl-carbamic acid ethyl ester

Downstream raw materials:

ethyl-phenyl-carbamic acid ethyl ester

carbon dioxide

hydrogen sulfide

N-ethyl-N-phenylamine