((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

Base Information

Chemical Name:((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane
CAS No.:1425925-91-2
Molecular Formula:C₂₃H₃₀O₃Si
Molecular Weight:382.575
Hs Code.:

Synonyms:((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

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Chemical Property of ((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

Chemical Property:

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Technology Process of ((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

There total 1 articles about ((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 110567-22-1
(2R,3S)-benzyloxy-2-benzyloxymethyl-6-oxabicyclo<3.1.0>hexane

: 1425925-91-2
((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

Guidance literature:: (2R,3S)-benzyloxy-2-benzyloxymethyl-6-oxabicyclo<3.1.0>hexane; With n-butyllithium; diisopropylamine; In hexane; tert-butyl methyl ether; at -15 - -10 ℃; for 1.66667h; Inert atmosphere;

chloro-trimethyl-silane; In hexane; tert-butyl methyl ether; at -10 - 0 ℃; for 0.5h;

Reference yield:

: 1425925-91-2
((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

: 1425925-92-3
(1S,3S,4S)-3-(benzyloxy)-4-(benzyloxymethyl)cyclopentanol

Guidance literature:: ((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane; With 5% palladium on barium sulfate; hydrogen; In tetrahydrofuran; at 20 ℃; for 18h; under 5171.62 Torr;

With hydrogenchloride; In water; ethyl acetate; for 1h;

Reference yield:

: 1425925-91-2
((1R,4S)-4-(benzyloxy)-3-(benzyioxymethyl)cyclopent-2-enyloxy)trimethylsilane

: 1425925-93-4
(1R,3S,4S)-3-(benzyloxy)-4-(benzyloxymethyl)cyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 5% palladium on barium sulfate; hydrogen / tetrahydrofuran / 18 h / 20 °C / 5171.62 Torr

1.2: 1 h

2.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 0 - 10 °C / Inert atmosphere

2.2: 20 h / 20 °C

2.3: 1 h / 20 °C

With 5% palladium on barium sulfate; hydrogen; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;