C₂₀H₁₄ClFN₂

Base Information

Chemical Name:C₂₀H₁₄ClFN₂
CAS No.:1590409-86-1
Molecular Formula:C₂₀H₁₄ClFN₂
Molecular Weight:336.796
Hs Code.:

C<sub>20</sub>H<sub>14</sub>ClFN<sub>2</sub>

Synonyms:C₂₀H₁₄ClFN₂

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Chemical Property of C₂₀H₁₄ClFN₂

Chemical Property:

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Technology Process of C₂₀H₁₄ClFN₂

There total 5 articles about C₂₀H₁₄ClFN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1590409-84-9
C₁₃H₈ClFN₂

: 100-39-0
benzyl bromide

: 1590409-86-1
C₂₀H₁₄ClFN₂

Guidance literature:: C₁₃H₈ClFN₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 16h;

Reference yield:

: 25391-59-7
5-iodo-3-nitro-pyridin-2-ol

: 1590409-86-1
C₂₀H₁₄ClFN₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: O-phenyl phosphorodichloridate / 0.5 h / 180 °C

2.1: tetrahydrofuran; 2-methyltetrahydrofuran / 1.25 h / -70 °C / Inert atmosphere

3.1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / Reflux

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

4.2: 16 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydride; potassium carbonate; O-phenyl phosphorodichloridate; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 6332-56-5
2-hydroxy-3-nitropyridine

: 1590409-86-1
C₂₀H₁₄ClFN₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sulfuric acid; periodic acid / water / 0.25 h / 90 °C

1.2: 0.33 h

2.1: O-phenyl phosphorodichloridate / 0.5 h / 180 °C

3.1: tetrahydrofuran; 2-methyltetrahydrofuran / 1.25 h / -70 °C / Inert atmosphere

4.1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / Reflux

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

5.2: 16 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; sodium hydride; potassium carbonate; acetic acid; O-phenyl phosphorodichloridate; periodic acid; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;