platinum(II) bis(benzonitrile)dichloride

Base Information

Chemical Name:platinum(II) bis(benzonitrile)dichloride
CAS No.:51921-56-3
Molecular Formula:2C₇H₅N*2Cl*Pt
Molecular Weight:472.233
Hs Code.:

Synonyms:platinum(II) bis(benzonitrile)dichloride

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Chemical Property of platinum(II) bis(benzonitrile)dichloride

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Technology Process of platinum(II) bis(benzonitrile)dichloride

There total 10 articles about platinum(II) bis(benzonitrile)dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

: 100-47-0
benzonitrile

: 10025-65-7
platinum(II) chloride

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

Guidance literature:: In benzonitrile; inert atmosphere; 100°C, 20 min; hot filtration (Celite), pptn. on addn. of hexanes, collection (filtration), washing (hexanes);
DOI:10.1016/s0020-1693(97)05642-9

Reference yield: 88.0%

: 100-47-0
benzonitrile

: 10025-65-7
platinum(II) chloride

: 14873-63-3,15617-19-3,51921-56-3
trans-bis(benzonitrile)dichloroplatinum(II)

Guidance literature:: In benzonitrile; suspn. of Pt compd. in benzonitrile was stirred at 100°C for 3 h; cooled to room temp.; petroleum ether added; filtered; washed (petrol ether); extd. (CH2Cl2); filtered; evapd.; chromd. (SiO2, CH2Cl2);
DOI:10.1039/b807410k

Reference yield: 80.0%

: 100-47-0
benzonitrile

: 10025-65-7
platinum(II) chloride

: 14873-63-3
cis-bis(benzonitrile)dichloroplatinum(II)

: 14873-63-3,15617-19-3,51921-56-3
trans-bis(benzonitrile)dichloroplatinum(II)

Guidance literature:: In neat (no solvent); refluxed at 100°C for 1 h; hot filtered, pumped to dryness, treated with hot benzene, filtered, residue washed (petroleum ether), dried under vacuo (yields the cis-isomer), the same procedure with the benzene-soln. gave the trans-isomer; elem. anal.;
DOI:10.1016/S0020-1693(00)84996-8