ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Base Information

Chemical Name:ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine
CAS No.:259219-20-0
Molecular Formula:C₂₂H₂₈N₂O₂
Molecular Weight:352.477
Hs Code.:

Synonyms:ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

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Chemical Property of ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

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Technology Process of ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

There total 3 articles about ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-03-6
ethyl iodide

: 188844-71-5
5,5,8,8-tetramethyl-N-(2-nitrophenyl)-5,6,7,8-tetrahydronaphthalen-2-amine

: 259219-20-0
ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Guidance literature:: 5,5,8,8-tetramethyl-N-(2-nitrophenyl)-5,6,7,8-tetrahydronaphthalen-2-amine; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h;

ethyl iodide; In N,N-dimethyl-formamide; for 1h;
DOI:10.1248/cpb.47.1778

Reference yield:

: 88-74-4
2-nitro-aniline

: 259219-20-0
ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / K₂CO₃; CuI / xylene / 14 h / 150 °C

2.1: NaH / dimethylformamide / 0.5 h

2.2: 100 percent / dimethylformamide / 1 h

With copper(l) iodide; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; xylene; 1.1: Substitution / 2.1: Metallation / 2.2: Alkylation;
DOI:10.1248/cpb.47.1778

Reference yield:

: 27452-17-1
6-bromo-1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene

: 259219-20-0
ethyl-(2-nitro-phenyl)-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / K₂CO₃; CuI / xylene / 14 h / 150 °C

2.1: NaH / dimethylformamide / 0.5 h

2.2: 100 percent / dimethylformamide / 1 h

With copper(l) iodide; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; xylene; 1.1: Substitution / 2.1: Metallation / 2.2: Alkylation;
DOI:10.1248/cpb.47.1778