methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

Base Information

Chemical Name:methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate
CAS No.:198274-51-0
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

Synonyms:methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

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Chemical Property of methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

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Technology Process of methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

There total 9 articles about methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 67-56-1
methanol

: 294872-90-5
3-[2-(carboxymethyl)-4-methoxy-6-methylphenyl]propionic acid

: 198274-51-0
methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

Guidance literature:: With sulfuric acid; at 65 ℃; for 5h;
DOI:10.1055/s-1997-983

Reference yield: 98.0%

: 67-56-1
methanol

: 294872-87-0
methyl 3-[2-(cyanomethyl)-4-methoxy-6-methylphenyl]propionate

: 198274-51-0
methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

Guidance literature:: With sulfuric acid; at 140 ℃; for 12h;

Reference yield:

: 874-63-5
3,5-dimethylmethoxybenzene

: 198274-51-0
methyl 3-{4-methoxy-2-[(methoxycarbonyl)methyl]-6-methylphenyl}propionate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / N-bromosuccinimide / acetonitrile / 12 h / 20 °C

2.1: 87 percent / N-bromosuccinimide; AIBN / CCl₄ / 2 h / Heating

3.1: 93 percent / dimethylformamide / 2 h / 90 °C

4.1: tri-o-tolylphosphane; triethylamine / [Pd(PPh₃)2]Cl₂ / toluene / 16 h / 165 °C

5.1: Mg / methanol / 6 h / 0 °C

5.2: 96 percent / KOH / methanol; H₂O / 24 h / 130 °C

6.1: 98 percent / conc. H₂SO₄ / 5 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sulfuric acid; magnesium; triethylamine; tris-(o-tolyl)phosphine; bis-triphenylphosphine-palladium(II) chloride; In methanol; tetrachloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: Bromination / 2.1: Bromination / 3.1: Substitution / 4.1: Heck coupling; olefination / 5.1: Reduction / 5.2: Hydrolysis / 6.1: Esterification;