O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate

Base Information

• Chemical Name: O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate
• CAS No.: 1110667-77-0
• Molecular Formula: C₂₅H₃₇NO₂SSi
• Molecular Weight: 443.726
• Mol file: 1110667-77-0.mol

Synonyms:O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate

Chemical Property of O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate

Chemical Property:

Purity/Quality:

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Technology Process of O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate

There total 1 articles about O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

6-{[tert-butyl(diphenyl)silyl]oxy}hexan-1-ol (121671-77-0) + dimethyl amine (124-40-3) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate (1110667-77-0)

Guidance literature:

6-{[tert-butyl(diphenyl)silyl]oxy}hexan-1-ol; 1,1'-Thiocarbonyldiimidazole;

dimethyl amine;

DOI:10.1055/s-0028-1083195

Reference yield: 81.0%

O-6-(tert-butyldimethylsiloxy)hexyl dimethylcarbamothioate (1110667-77-0) → t-butyl diphenylsilanol (93547-88-7) + ((6-bromohexyl)oxy)(tert-butyl)diphenylsilane (172995-33-4)

Guidance literature:

With 4-(bromomethylene)morpholin-4-ium bromide; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1055/s-0028-1083195

upstream raw materials:

6-{[tert-butyl(diphenyl)silyl]oxy}hexan-1-ol

dimethyl amine

1,1'-Thiocarbonyldiimidazole

Downstream raw materials:

t-butyl diphenylsilanol

((6-bromohexyl)oxy)(tert-butyl)diphenylsilane