2-oxopropionic acid 4-acetylaminobenzyl ester

Base Information

Chemical Name:2-oxopropionic acid 4-acetylaminobenzyl ester
CAS No.:246237-18-3
Molecular Formula:C₁₂H₁₃NO₄
Molecular Weight:235.24
Hs Code.:

Synonyms:2-oxopropionic acid 4-acetylaminobenzyl ester

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Chemical Property of 2-oxopropionic acid 4-acetylaminobenzyl ester

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Technology Process of 2-oxopropionic acid 4-acetylaminobenzyl ester

There total 1 articles about 2-oxopropionic acid 4-acetylaminobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 16375-88-5
N-(4-hydroxymethylphenyl)acetamide

: 5704-66-5
pyruvoyl chloride

: 246237-18-3
2-oxopropionic acid 4-acetylaminobenzyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ja991507g

Reference yield: 85.0%

: 67-64-1
acetone

: 246237-18-3
2-oxopropionic acid 4-acetylaminobenzyl ester

: 2-hydroxy-2-methyl-4-oxopentanoic acid 4-acetylaminobenzyl ester

Guidance literature:: acetone; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 0.5h;

2-oxopropionic acid 4-acetylaminobenzyl ester; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 0.5h;
DOI:10.1021/ja991507g

Reference yield:

: 67-64-1
acetone

: 246237-18-3
2-oxopropionic acid 4-acetylaminobenzyl ester

: (R)-2-hydroxy-2-methyl-4-oxopentanoic acid 4-acetylaminobenzyl ester

: (S)-2-Hydroxy-2-methyl-4-oxo-pentanoic acid 4-acetylamino-benzyl ester

Guidance literature:: acetone; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 0.5h;

2-oxopropionic acid 4-acetylaminobenzyl ester; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 0.5h;

With aldolase antibody 38C₂; In phosphate buffer; pH=7.4; Title compound not separated from byproducts;
DOI:10.1021/ja991507g