5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Base Information

Chemical Name:5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine
CAS No.:512779-26-9
Molecular Formula:C₂₉H₃₆N₂O₇Si
Molecular Weight:552.7
Hs Code.:

Synonyms:5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Suppliers and Price of 5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

There total 7 articles about 5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 213552-29-5
5'-O-tert-butyldiphenylsilyl-2',3'-O-isopropylideneuridine

: 512779-26-9
5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Guidance literature:: With potassium hydroxide; for 0.05h; microwave irradiation;
DOI:10.1055/s-2002-35592

Reference yield:

: 5-bromomethyl-1-[6-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl]-1H-pyrimidine-2,4-dione

: 512779-26-9
5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1016/j.tetlet.2006.09.083

Reference yield:

: 917482-61-2
2',3'-isopropylidene-5-methyl-5'-O-t-butyldiphenylsilyluridine

: 512779-26-9
5'-O-tert-butyldiphenylsilyl-5-hydroxymethyl-2',3'-O-isopropylideneuridine

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide; benzoyl peroxide / CCl₄ / Heating

2: 491 mg / NaHCO₃ / H₂O; tetrahydrofuran / 20 °C

With N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; water;
DOI:10.1016/j.tetlet.2006.09.083