1,1-dimethylbutyl 2,2-dimethylpropaneperoxoate

Base Information

• Chemical Name: 1,1-dimethylbutyl 2,2-dimethylpropaneperoxoate
• CAS No.: 118364-97-9
• Molecular Formula: C₁₁H₂₂O₃
• Molecular Weight: 202.294
• Mol file: 118364-97-9.mol

Synonyms:2-(n-propyl)-2-propyl peroxypivalate

Chemical Property of 1,1-dimethylbutyl 2,2-dimethylpropaneperoxoate

Chemical Property:

• Vapor Pressure: 0.0907mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-dimethylbutyl 2,2-dimethylpropaneperoxoate

There total 1 articles about 1,1-dimethylbutyl 2,2-dimethylpropaneperoxoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylbutyl hydroperoxide (13393-68-5) + pivaloyl chloride (3282-30-2) → 2-(n-propyl)-2-propyl peroxypivalate (118364-97-9)

Guidance literature:

With potassium hydroxide; In water; Petroleum ether; for 0.5h;

DOI:10.1246/bcsj.61.1641

Reference yield:

2-(n-propyl)-2-propyl peroxypivalate (118364-97-9) → 2-methylpentan-2-ol (590-36-3) + acetone (67-64-1)

Guidance literature:

In various solvent(s); at 60 ℃; for 50h; Product distribution;

DOI:10.1246/bcsj.61.1641

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-2-yloxoyl radical (80037-90-7) + 2-(n-propyl)-2-propyl peroxypivalate (118364-97-9) → 2-methoxy-1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole (80037-95-2) + 1,1,3,3-Tetramethyl-2-propoxy-2,3-dihydro-1H-isoindole + 2-Methyl-5-(1,1,3,3-tetramethyl-1,3-dihydro-isoindol-2-yloxy)-pentan-2-ol + 1,1,3,3-Tetramethyl-2-(1-phenyl-pentyloxy)-2,3-dihydro-1H-isoindole + 2-Methyl-7-phenyl-7-(1,1,3,3-tetramethyl-1,3-dihydro-isoindol-2-yloxy)-heptan-2-ol + 2-[2-(tert-hexyloxy)-1-phenylethoxy]-1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole

Guidance literature:

at 60 ℃; for 1h; Product distribution;

DOI:10.1021/jo9707489

upstream raw materials:

1,1-dimethylbutyl hydroperoxide

pivaloyl chloride

Downstream raw materials:

2-methylpentan-2-ol

acetone

2-methoxy-1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindole