4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

Base Information

Chemical Name:4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide
CAS No.:120780-15-6
Molecular Formula:C₁₉H₂₃NOSSi
Molecular Weight:341.549
Hs Code.:

4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ<sup>4</sup>-benzo[c][1,2]thiazine 2-oxide

Synonyms:4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

There total 2 articles about 4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6224-91-5
trimethyl(prop-1-ynyl)silane

: 123552-85-2
N-phenyl-S-(4-methylphenyl)sulfoximidoyl chloride

: 120780-15-6
4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

Guidance literature:: With aluminium trichloride; In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4039(00)96846-1

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 120780-16-7
4-Methyl-2-p-tolyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

: 120780-15-6
4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

: 120780-28-1
4-Methyl-2-(4-methyl-2-trimethylsilanyl-phenyl)-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

Guidance literature:: With n-butyllithium; Product distribution; 1.) THF, -78 deg C, 15 min; quenching with various electrophiles;
DOI:10.1016/S0040-4039(00)80723-6

Reference yield: 81.0%

: 120780-15-6
4-Methyl-2-p-tolyl-3-trimethylsilanyl-2λ⁴-benzo[c][1,2]thiazine 2-oxide

: 52562-19-3
2-isopropenylaniline

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In tetrahydrofuran; methanol; for 15h; Ambient temperature;
DOI:10.1055/s-1995-3986