acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

Base Information

Chemical Name:acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester
CAS No.:1556019-50-1
Molecular Formula:C₁₅H₂₂BrNO₂SSi
Molecular Weight:388.401
Hs Code.:

Synonyms:acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

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Chemical Property of acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

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Technology Process of acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

There total 7 articles about acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174731-67-9
3-bromo-4-(2-oxopropyl)-N-trimethylsilanylmethylthiobenzamide

: 74-88-4
methyl iodide

: 1556019-50-1
acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 4h;

Reference yield:

: 1556019-48-7
3-bromo-4-formyl-N-[(trimethylsilyl)methyl]benzamide

: 1556019-50-1
acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol / 1 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

3: Lawessons reagent / tetrahydrofuran / 3 h / Reflux

4: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 °C

With Lawessons reagent; sodium tetrahydroborate; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 1556019-47-6
3-bromo-4-(dibromomethyl)-N-[(trimethylsilyl)methyl]benzamide

: 1556019-50-1
acetic acid 2-bromo-4{methylsulfanyl-[(E)-trimethylsilanylmethylimino]-methyl}-benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: silver nitrate / water; acetone / 6 h / 20 °C

2: sodium tetrahydroborate / methanol / 1 h / 20 °C

3: triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

4: Lawessons reagent / tetrahydrofuran / 3 h / Reflux

5: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 °C

With Lawessons reagent; sodium tetrahydroborate; potassium carbonate; silver nitrate; triethylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;