acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

Base Information

Chemical Name:acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique
CAS No.:117570-39-5
Molecular Formula:C₁₈H₂₄O₆
Molecular Weight:336.385
Hs Code.:

Synonyms:acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

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Chemical Property of acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

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Technology Process of acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

There total 7 articles about acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 117570-38-4
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

: 117570-39-5
acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

Guidance literature:: In methanol; at 95 ℃; for 5h;
DOI:10.1016/S0040-4020(01)85896-8

Reference yield:

: 930-68-7
cyclohexenone

: 117570-39-5
acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-butyllithium / 1.) THF, r.t., 2 h; 2.) THF, 48 h, 20 deg C

2: 93 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

4: 36 percent / propionic acid / 5 h / 135 °C

5: 100 percent / methanol / 5 h / 95 °C

With lithium aluminium tetrahydride; n-butyllithium; propionic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85896-8

Reference yield:

: 3688-89-9
bis-methoxymethylenoxy-1,2 benzene

: 117570-39-5
acide (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetique

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-butyllithium / 1.) THF, r.t., 2 h; 2.) THF, 48 h, 20 deg C

2: 93 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

4: 36 percent / propionic acid / 5 h / 135 °C

5: 100 percent / methanol / 5 h / 95 °C

With lithium aluminium tetrahydride; n-butyllithium; propionic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85896-8