(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

Base Information

Chemical Name:(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle
CAS No.:117570-38-4
Molecular Formula:C₂₀H₂₈O₆
Molecular Weight:364.439
Hs Code.:

Synonyms:(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

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Chemical Property of (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

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Technology Process of (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

There total 6 articles about (bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 78-39-7
Triethyl orthoacetate

: 108275-25-8
(bis-methoxymethylenoxy-2',3' phenyl)-3 cyclohexene-2 ol-1

: 117570-38-4
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

Guidance literature:: With propionic acid; at 135 ℃; for 5h;
DOI:10.1016/S0040-4020(01)85896-8

Reference yield:

: 930-68-7
cyclohexenone

: 117570-38-4
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-butyllithium / 1.) THF, r.t., 2 h; 2.) THF, 48 h, 20 deg C

2: 93 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

4: 36 percent / propionic acid / 5 h / 135 °C

With lithium aluminium tetrahydride; n-butyllithium; propionic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)85896-8

Reference yield:

: 3688-89-9
bis-methoxymethylenoxy-1,2 benzene

: 117570-38-4
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 acetate d'ethyle

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-butyllithium / 1.) THF, r.t., 2 h; 2.) THF, 48 h, 20 deg C

2: 93 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 100 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

4: 36 percent / propionic acid / 5 h / 135 °C

With lithium aluminium tetrahydride; n-butyllithium; propionic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)85896-8