N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

Base Information

Chemical Name:N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid
CAS No.:127817-89-4
Molecular Formula:C₁₈H₁₇ClF₃NO₃
Molecular Weight:387.786
Hs Code.:

Synonyms:N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

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Technology Process of N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

There total 3 articles about N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 50424-99-2
2-chloro-4-methoxybenzoic acid chloride

: 117730-46-8
N-(1,1,1-trifluoro-2-propyl)-4-methoxyaniline

: 127817-89-4
N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

Guidance literature:: With potassium carbonate; at 80 ℃; for 2h;
DOI:10.1002/ardp.19903230204

Reference yield:

: 41068-36-4
2-chloro-4-methoxyacetophenone

: 127817-89-4
N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / Br₂, NaOH / dioxane / 4 h / 60 °C

2: 82 percent / SOCl₂ / Heating

3: 69 percent / K₂CO₃ / 2 h / 80 °C

With sodium hydroxide; thionyl chloride; bromine; potassium carbonate; In 1,4-dioxane;
DOI:10.1002/ardp.19903230204

Reference yield:

: 21971-21-1
2-chloro-4-methoxybenzoic acid

: 127817-89-4
N-(4-Methoxyphenyl)-N-(1,1,1-trifluor-2-propyl)-2-chlor-4-methoxybenzamid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / SOCl₂ / Heating

2: 69 percent / K₂CO₃ / 2 h / 80 °C

With thionyl chloride; potassium carbonate;
DOI:10.1002/ardp.19903230204