O,O'-diethyl cyclohexylthiophosphonate

Base Information

Chemical Name:O,O'-diethyl cyclohexylthiophosphonate
CAS No.:73178-34-4
Molecular Formula:C₁₀H₂₁O₂PS
Molecular Weight:236.315
Hs Code.:

Synonyms:O,O'-diethyl cyclohexylthiophosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O'-diethyl cyclohexylthiophosphonate

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Technology Process of O,O'-diethyl cyclohexylthiophosphonate

There total 6 articles about O,O'-diethyl cyclohexylthiophosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.6%

: 999-01-9
O,O'-diethyl thiophosphonate

: 110-83-8
cyclohexene

: 73178-34-4
O,O'-diethyl cyclohexylthiophosphonate

Guidance literature:: With alkali metal diethyl thiophosphite; alkali metal perchlorate; In acetonitrile; Electrolysis;

Reference yield:

: 542-18-7
cyclohexyl chloride

: 73178-34-4
O,O'-diethyl cyclohexylthiophosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) PCl₃, anhydrous Al₂Cl₆, 2.) Thiourea, H₂O / CH₂Cl₂

2: ethanol

With aluminium chloride dimer; water; thiourea; phosphorus trichloride; In ethanol;
DOI:10.1021/jo01299a053