tert-Butyl N-(methylsulfamoyl)carbamate

Base Information

Chemical Name:tert-Butyl N-(methylsulfamoyl)carbamate
CAS No.:125987-94-2
Molecular Formula:C₆H₁₄N₂O₄S
Molecular Weight:210.254
Hs Code.:
Mol file:125987-94-2.mol

Synonyms:Carbamicacid, [(methylamino)sulfonyl]-, 1,1-dimethylethyl ester (9CI); tert-ButylN-(methylsulfamoyl)carbamate; tert-Butyl N-[(methylamino)sulfonyl]carbamate

Suppliers and Price of tert-Butyl N-(methylsulfamoyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
TERT-BUTYL N-(METHYLSULFAMOYL)CARBAMATE 95.00%
5MG
$ 503.36

Total 7 raw suppliers

Chemical Property of tert-Butyl N-(methylsulfamoyl)carbamate

Chemical Property:

PSA：96.37000
Density:1.238g/cm³
LogP:1.65140

Purity/Quality:

99% ^*data from raw suppliers

TERT-BUTYL N-(METHYLSULFAMOYL)CARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-Butyl N-(methylsulfamoyl)carbamate

There total 4 articles about tert-Butyl N-(methylsulfamoyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 75-65-0
tert-butyl alcohol

: 125987-94-2
N-(tert-butoxycarbonyl)-N'-(methyl)sulfamide

Guidance literature:: isocyanate de chlorosulfonyle; tert-butyl alcohol; With triethylamine; In dichloromethane; for 0.5h; Inert atmosphere;

With SULFAMIDE; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201700783

Reference yield: 97.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 74-89-5
methylamine

: 75-65-0
tert-butyl alcohol

: 125987-94-2
N-(tert-butoxycarbonyl)-N'-(methyl)sulfamide

Guidance literature:: isocyanate de chlorosulfonyle; tert-butyl alcohol; In toluene; at 0 ℃; for 0.5h;

With pyridine; In toluene; at 0 ℃; for 1h;

methylamine; In water; toluene; at 0 ℃; for 2h; Further stages.;
DOI:10.1016/j.tetlet.2004.01.008

Reference yield:

: 147000-89-3
N-tert-butyloxycarbonylsulfamoyl chloride

: 74-89-5
methylamine

: 125987-94-2
N-(tert-butoxycarbonyl)-N'-(methyl)sulfamide

Guidance literature:: N-tert-butyloxycarbonylsulfamoyl chloride; With pyridine; In toluene; Cooling;

methylamine; In water; toluene; Cooling;
DOI:10.1016/j.tetasy.2013.04.006