2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

Base Information

Chemical Name:2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid
CAS No.:1451149-86-2
Molecular Formula:C₁₉H₂₃N₃O₃S
Molecular Weight:373.476
Hs Code.:

Synonyms:2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

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Chemical Property of 2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

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Technology Process of 2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

There total 4 articles about 2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1451149-80-6
(2E,4E)-5-(benzo[d][1,3]dioxol-5-yl)penta-2,4-dienehydrazide

: 1122-82-3
isothiocyanatocyclohexane

: 1451149-86-2
2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

Guidance literature:: In ethanol; for 0.5h; Microwave irradiation;
DOI:10.3390/molecules18066366

Reference yield:

: 136-72-1
piperic acid

: 1451149-86-2
2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2: hydrazine hydrate / dichloromethane / 0.5 h / 20 °C / Cooling with ice

3: ethanol / 0.5 h / Microwave irradiation

With oxalyl dichloride; hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.3390/molecules18066366

Reference yield:

: 4711-72-2
piperic acid chloride

: 1451149-86-2
2-[(2E,4E)-5-(1,3-benzodioxol-5-yl)penta-2,4-dienoyl]-N-cyclohexylhydrazinecarbothioamid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / dichloromethane / 0.5 h / 20 °C / Cooling with ice

2: ethanol / 0.5 h / Microwave irradiation

With hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.3390/molecules18066366