N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

Base Information

Chemical Name:N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide
CAS No.:1237587-41-5
Molecular Formula:C₂₀H₁₄Cl₃F₆N₃O₂
Molecular Weight:548.699
Hs Code.:

Synonyms:N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

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Chemical Property of N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

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Technology Process of N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

There total 11 articles about N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41463-83-6
3,3,3-trifluoropropanoyl chloride

: 1237587-92-6
N-methyl-N-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}hydrazine

: 1237587-41-5
N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-41-5
N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 0.83 h / 75 °C

3.1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

4.2: 1 h / 20 °C

5.1: potassium carbonate; methanol / 3 h / 20 °C

6.1: hydrogenchloride / water; tetrahydrofuran / 0.17 h / 20 °C

6.2: 1 h / 0 °C

7.1: zinc; water; acetic acid / ethanol; tetrahydrofuran / 3 h / 20 °C

8.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; methanol; N-chloro-succinimide; water; iron; sodium hydride; potassium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 66399-01-7
2-chloro-5-hydroxyiminomethylnitrobenzene

: 1237587-41-5
N′-methyl-N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}-3,3,3-trifluoropropionohydrazide

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 0.83 h / 75 °C

3.1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

4.2: 1 h / 20 °C

5.1: potassium carbonate; methanol / 3 h / 20 °C

6.1: hydrogenchloride / water; tetrahydrofuran / 0.17 h / 20 °C

6.2: 1 h / 0 °C

7.1: zinc; water; acetic acid / ethanol; tetrahydrofuran / 3 h / 20 °C

8.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; methanol; N-chloro-succinimide; water; iron; sodium hydride; potassium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;