2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

Base Information

Chemical Name:2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene
CAS No.:220416-57-9
Molecular Formula:C₁₉H₂₈Cl₂O
Molecular Weight:343.337
Hs Code.:

Synonyms:2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

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Chemical Property of 2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

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Technology Process of 2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

There total 1 articles about 2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 79-01-6
Trichloroethylene

: 102225-88-7
(-)-(S)-1-(2,4,6-triisopropylphenyl)ethanol

: 220416-57-9
2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

Guidance literature:: (S)-(-)-1-(2,4,6-triisopropylphenyl)ethanol; With potassium hydroxide; In tetrahydrofuran; pentane; at 0 - 20 ℃; for 2h; Inert atmosphere;

Trichloroethylene; In tetrahydrofuran; pentane; at -50 - 20 ℃; for 2h;
DOI:10.1021/acs.orglett.6b01058

Reference yield: 88.0%

: 220416-57-9
2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

: 74-88-4
methyl iodide

: 1332863-37-2
(S,E)-2-(1-(1,2-dichloroprop-1-enyloxy)ethyl)-1,3,5-triisopropylbenzene

Guidance literature:: 2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

methyl iodide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at -90 - 20 ℃;
DOI:10.1007/s10870-011-0045-3

Reference yield: 81.0%

: 220416-57-9
2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene

: 1240520-79-9
(S)-O-vinyl-1-(2,4,6-triisopropylphenyl)ethanol

Guidance literature:: 2-((1S)-1-((1E)-1,2-dichloroethenyloxy)ethyl)-1,3,5-triisopropylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -55 ℃; for 0.166667h; Inert atmosphere;

With pyridine; rosenmund catalyst; hydrogen; at 20 ℃;
DOI:10.1021/acs.orglett.6b01058