Trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane

Base Information

Chemical Name:Trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane
CAS No.:154557-38-7
Molecular Formula:C₁₂H₃₂O₂Si₃
Molecular Weight:292.641
Hs Code.:
DSSTox Substance ID:DTXSID00400440
Mol file:154557-38-7.mol

Synonyms:154557-38-7;trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane;1-(TRIMETHYLSILYL)-2,3-BIS(TRIMETHYLSILYLOXY)PROPANE;DTXSID00400440;ZGNPKKBNNSGISB-UHFFFAOYSA-N

Suppliers and Price of Trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane

Chemical Property:

Refractive Index:n20/D 1.424(lit.)
Boiling Point:182 °C(lit.)
Flash Point:187 °F
PSA：18.46000
Density:0.848 g/mL at 25 °C(lit.)
LogP:4.39620
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:292.17100986
Heavy Atom Count:17
Complexity:223

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)CC(CO[Si](C)(C)C)O[Si](C)(C)C

Technology Process of Trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane

There total 2 articles about Trimethyl-(1-trimethylsilyl-3-trimethylsilyloxypropan-2-yl)oxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 75-77-4
chloro-trimethyl-silane

: 119235-89-1
3-(trimethylsilyl)-1,2-propanediol

: 154557-38-7
2,3-bis(trimethylsilyloxy)-trimethylsilylpropane

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4039(00)79941-2

Reference yield:

: 762-72-1
allyl-trimethyl-silane

: 154557-38-7
2,3-bis(trimethylsilyloxy)-trimethylsilylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / N-methylmorpholine N-oxide / 4percent aq. OsO₄ / acetone / 0 deg C, 30 min; RT, 1 h

2: 89 percent / pyridine / CH₂Cl₂ / 0 °C

With pyridine; 4-methylmorpholine N-oxide; osmium(VIII) oxide; In dichloromethane; acetone;
DOI:10.1016/S0040-4039(00)79941-2

Reference yield: 100.0%

: 100-52-7
benzaldehyde

: 154557-38-7
2,3-bis(trimethylsilyloxy)-trimethylsilylpropane

: Trimethyl-(2-phenyl-[1,3]dioxolan-4-ylmethyl)-silane

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 2h; Product distribution; var. oxo compounds;
DOI:10.1016/S0040-4039(00)79941-2